136918-14-4合成路线 （共 708 条）
反应条件
1: 78 percent / K2CO3 / dimethylsulfoxide / Heating; 25 deg C, overnight; 55 deg C, 6 h
2: 82 percent / CrO3, pyridine / CH2Cl2 / 0.5 h / 25 °C
View Scheme
参考文献
Wada, Masao; Nakai, Hideo; Sato, Yasuhiko; Hatanaka, Yasumaru; Kanaoka, Yuichi
Tetrahedron, 1983 , vol. 39, # 16 p. 2691 - 2698
反应条件
in methanol
0.166667 h; Ambient temperature;
参考文献
Varma; Kapoor
Pharmazie, 1980 , vol. 35, # 2 p. 78 - 80
反应条件
1: With di-isopropyl azodicarboxylate; triphenylphosphine
Gabriel synthesis; Inert atmosphere;
2: With hydrazine hydrate
Gabriel synthesis; Inert atmosphere;
3: With hydrogenchloride in water
Inert atmosphere;
参考文献
Tuchscherer, Andre; Schaarschmidt, Dieter; Schulze, Steffen; Hietschold, Michael; Lang, Heinrich
European Journal of Inorganic Chemistry, 2011 , # 28 p. 4421 - 4428
参考文献
Beis
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 139, p. 62
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=80°C; Substitution; 18 h;
参考文献
Ossipov, Dimitri; Zamaratski, Edouard; Chattopadhyava, Jyoti
Helvetica Chimica Acta, 1999 , vol. 82, # 12 p. 2186 - 2200
反应条件
DMEAD; triphenylphosphine in tetrahydrofuran
T=20°C; Mitsunobu reaction;
参考文献
Hagiya, Kazutake; Muramoto, Natsuko; Misaki, Tomonori; Sugimura, Takashi
Tetrahedron, 2009 , vol. 65, # 31 p. 6109 - 6114
反应条件
triethylamine; 3-diphenyloxyphosphinyl-2-oxazolidinone in acetonitrile
T=40°C; 0.5 h;
参考文献
Abdel-Aziz, Alaa A.-M.
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 5 p. 614 - 626
反应条件
2,6-bis(1,1-dimethylethyl)-p-benzoquinone in dichloromethane
T=20°C; 1 h;
参考文献
Mukaiyama, Teruaki; Aoki, Hidenori
Chemistry Letters, 2005 , vol. 34, # 2 p. 142 - 143
反应条件
sodium hydroxide in water; acetonitrile
11 h; Irradiation;
参考文献
Suau, Rafael; Garcia-Segura, Rafael; Sanchez-Sanchez, Cristobal; Perez-Inestrosa, Ezequiel; Pedraza, Ana Maria
Tetrahedron, 2003 , vol. 59, # 16 p. 2913 - 2919
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
26 h; Ambient temperature;
参考文献
Moody, Christopher J.; Rahimtoola, Kulsum F.; Porter, Barry; Ross, Barry C.
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2105 - 2114
