136918-14-4合成路线 （共 708 条）
反应条件
1: With pyridine in acetonitrile
2: With bromine in acetonitrile
参考文献
Bozkurt, Yasemin Soydas; Kutuk, Halil
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 11 p. 2250 - 2257
反应条件
bromine in pyridine; acetonitrile
T=0°C; 2 h;
参考文献
Klose, Jana; Reese, Colin B.; Song, Quanlai
Tetrahedron, 1997 , vol. 53, # 42 p. 14411 - 14416
反应条件
in acetonitrile
T=60°C; 0.25 h;
参考文献
Kita, Yasuyuki; Haruta, Jun-ichi; Fujii, Takehiko; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1981 , # 6 p. 451 - 452
反应条件
triethylamine in dichloromethane
6 h; Heating;
参考文献
Chun; Park; Oh; Hong; Kim
Synthesis, 1994 , # 9 p. 909 - 910
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C;
参考文献
Wang, You-Qing; Lu, Sheng-Mei; Zhou, Yong-Gui
Organic Letters, 2005 , vol. 7, # 15 p. 3235 - 3238
反应条件
pyridine; oxonium; bromine
参考文献
Davis, Anthony P.; Whitham, Gordon H.
Journal of the Chemical Society, Chemical Communications, 1981 , # 15 p. 741 - 742
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=20°C;
参考文献
Bojarski, Andrzej J.; Duszynska, Beata; Kolaczkowski, Marcin; Kowalski, Piotr; Kowalska, Teresa
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 23 p. 5863 - 5866
反应条件
1: 78 percent / K2CO3 / dimethylsulfoxide / Heating; 25 deg C, overnight; 55 deg C, 6 h
2: 82 percent / CrO3, pyridine / CH2Cl2 / 0.5 h / 25 °C
3: 68 percent / BF3-etherate / diethyl ether / 25 °C
4: 56 percent / acetone / 0.42 h / 10 - 20 °C / Irradiation
5: 49 percent / Raney Ni / ethanol / 2 h / Heating
View Scheme
参考文献
Wada, Masao; Nakai, Hideo; Sato, Yasuhiko; Hatanaka, Yasumaru; Kanaoka, Yuichi
Tetrahedron, 1983 , vol. 39, # 16 p. 2691 - 2698
反应条件
1: 78 percent / K2CO3 / dimethylsulfoxide / Heating; 25 deg C, overnight; 55 deg C, 6 h
2: 82 percent / CrO3, pyridine / CH2Cl2 / 0.5 h / 25 °C
3: 68 percent / BF3-etherate / diethyl ether / 25 °C
View Scheme
参考文献
Wada, Masao; Nakai, Hideo; Sato, Yasuhiko; Hatanaka, Yasumaru; Kanaoka, Yuichi
Tetrahedron, 1983 , vol. 39, # 16 p. 2691 - 2698
反应条件
1: triton B / ethyl acetate / Heating
2: PTSA / toluene / Heating
View Scheme
参考文献
Islam; Raphael
Journal of the Chemical Society, 1955 , p. 3151,3153
