136918-14-4合成路线 （共 708 条）
反应条件
dirhodium tetraacetate in dichloromethane
T=20°C; 7 h;
参考文献
Nikolaev, Vsevolod V.; Heimgartner, Heinz; Linden, Anthony; Krylov, Ivan S.; Nikolaev, Valerij A.
European Journal of Organic Chemistry, 2006 , # 20 p. 4737 - 4746
反应条件
in N,N-dimethyl-formamide
2 h; Ambient temperature;
参考文献
Consonni, Piero; Favara, Duccio; Omodei-Sale, Amedeo; Bartolini, Giuseppe; Ricci, Alfredo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 967 - 974
反应条件
1: 78 percent / K2CO3 / dimethylsulfoxide / Heating; 25 deg C, overnight; 55 deg C, 6 h
2: 82 percent / CrO3, pyridine / CH2Cl2 / 0.5 h / 25 °C
3: 59 percent / BF3-etherate / diethyl ether / 25 °C
View Scheme
参考文献
Wada, Masao; Nakai, Hideo; Sato, Yasuhiko; Hatanaka, Yasumaru; Kanaoka, Yuichi
Tetrahedron, 1983 , vol. 39, # 16 p. 2691 - 2698
反应条件
in ethanol
1 h; Heating;
参考文献
Spiessens, Luc I.; Anteunis, Marc J. O.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 11-12 p. 965 - 994
反应条件
potassium carbonate in ethanol
参考文献
Nycomed Imaging AS
Patent: US5531978 A1, 1996 ;
Title/Abstract Full Text Show Details
Nycomed Imaging AS
Patent: US5198208 A1, 1993 ;
反应条件
1: alcohol; hydrazine hydrate
2: 160 °C / weiteres Edukt Nitrobenzol.
View Scheme
参考文献
Drew; Hatt
Journal of the Chemical Society, 1937 , p. 16,25
反应条件
triethylamine; copper diacetate in dichloromethane
T=20°C; Chan-Lam Coupling; 120 h;
参考文献
Eisai Co., Ltd.
Patent: US2007/72896 A1, 2007 ;
Location in patent: Page/Page column 54 ;
反应条件
potassium carbonate in ethanol
16 h; Heating;
参考文献
Ahmed; Stratford; Jenkins
Arzneimittel-Forschung/Drug Research, 1985 , vol. 35, # 12 p. 1763 - 1768
参考文献
Hankovszky; Hideg; Bodi; Frank
Journal of Medicinal Chemistry, 1986 , vol. 29, # 7 p. 1138 - 1152
反应条件
potassium carbonate in ethanol
4 h; Heating;
参考文献
Ahmed; Stratford; Jenkins
Arzneimittel-Forschung/Drug Research, 1985 , vol. 35, # 12 p. 1763 - 1768
