136918-14-4合成路线 （共 708 条）
反应条件
1: HNO3+H2SO4 / Darstellung; Nitrierung
2: SnCl2; aqueous HCl
3: sodium nitrite; concentrated sulfuric acid / Beim Erwaermen des Reaktionsgemisches mit Wasser und Erwaermen des Reaktionsprodukts mit Ammoniumacetat in Essigsaeure
View Scheme
参考文献
Levy; Stephen
Journal of the Chemical Society, 1931 , p. 79,81
反应条件
18-crown-6 ether; potassium tert-butylate in dimethyl sulfoxide
3 h; Irradiation;
参考文献
Maquieira, Manuel Bajo; Penenory, Alicia B.; Rossi, Roberto A.
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 1012 - 1015
反应条件
1,4-diaza-bicyclo[2.2.2]octane; potassium iodide in dimethylsulfoxide-d6
T=35 - 40°C; 35 h; Irradiation;
参考文献
Russell, Glen A.; Chen, Ping; Kim, Byeong Hyo; Rajaratnam, Ragine
Journal of the American Chemical Society, 1997 , vol. 119, # 38 p. 8795 - 8801
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,1,1,2,2,2-hexabutyl-distannane in benzene
T=60°C; 60 h; Irradiation;
参考文献
Wang, Chen; Russell, Glen A.; Trahanovsky, Walter S.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9956 - 9959
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,1,1,2,2,2-hexabutyl-distannane in benzene
T=60°C; 20 h; Irradiation;
参考文献
Wang, Chen; Russell, Glen A.; Trahanovsky, Walter S.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9956 - 9959
反应条件
potassium carbonate in N,N-dimethyl-formamide
20 h;
参考文献
Lokaj, Jan; Kettmann, Viktor; Marchalin, Stefan; Sikoraiova, Jana
Acta Crystallographica Section C: Crystal Structure Communications, 2001 , vol. 57, # 6 p. 735 - 736
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=20°C; Mitsunobu reaction; 3 h;
参考文献
Leonard, Kristi; Marugan, Juan Jose; Raboisson, Pierre; Calvo, Raul; Gushue, Joan M.; Koblish, Holly K.; Lattanze, Jennifer; Zhao, Shuyuan; Cummings, Maxwell D.; Player, Mark R.; Maroney, Anna C.; Lu, Tianbao
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 13 p. 3463 - 3468
反应条件
pyridine; methanol; N-benzyl-trimethylammonium hydroxide
anschliessenden Behandeln mit Malonsaeure und Piperidin;
参考文献
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
反应条件
1: K2CO3, n-Bu4NBr / acetone / 24 h / Ambient temperature
2: NaI / acetone / Ambient temperature
View Scheme
参考文献
Prabhakar; Kumar, N. Vasanth; Reddy, M. Ravikanth; Sarma; Reddy, G. Om
Organic Process Research and Development, 1999 , vol. 3, # 3 p. 155 - 160
反应条件
1: K2CO3, n-Bu4NBr / acetone / 24 h / Ambient temperature
2: NaI / acetone / Ambient temperature
View Scheme
参考文献
Ha, Deok-Chan; Yun, Chang-Soo; Yu, Eunsun
Tetrahedron Letters, 1996 , vol. 37, # 15 p. 2577 - 2580
