136918-14-4合成路线 （共 708 条）
参考文献
Hoechster Farbw.
Patent: DE127138 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 6, p. 156
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Mohr
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2>79, p. 281
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2>80, p. 1,14,18,22
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Meyer
Chemische Berichte, 1906 , vol. 39, p. 1451
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Mohr; Koehler
Chemische Berichte, 1906 , vol. 39, p. 1057
反应条件
1: lithium alanate; diethyl ether
2: chlorocarbonic acid ethyl ester; aq. NaOH solution
View Scheme
参考文献
Dunet et al.
Bulletin de la Societe Chimique de France, 1950 , p. 877,878
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C;
参考文献
Kowalski, Piotr; Mitka, Katarzyna; Jaskowska, Jolanta; Duszynska, Beata; Bojarski, Andrzej J.
Archiv der Pharmazie, 2013 , vol. 346, # 5 p. 339 - 348
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; Alkylation; 8 h;
参考文献
Cho, Su-Dong; Kim, Hyeung-Jae; Ahn, Chuljin; Falckb; Shin, Dong-Soo
Tetrahedron Letters, 1999 , vol. 40, # 47 p. 8215 - 8217
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=25°C; Mitsunobu reaction; 17 h;
参考文献
Baumgartner, Corinne; Eberle, Christian; Diederich, Francois; Lauw, Susan; Rohdich, Felix; Eisenreich, Wolfgang; Bacher, Adelbert
Helvetica Chimica Acta, 2007 , vol. 90, # 6 p. 1043 - 1068
反应条件
triphenylphosphine in toluene
T=110°C; 48 h; Inert atmosphere;
参考文献
De Los Santos, Jesus M.; Ochoa, Zelai; Palacios, Francisco
Arkivoc, 2012 , vol. 2012, # 4 p. 54 - 62
参考文献
Gabriel; Ohle
Chemische Berichte, 1917 , vol. 50, p. 823
反应条件
potassium carbonate in acetonitrile
48 h; Inert atmosphereReflux;
参考文献
Zhou, Liang
Journal of Chemical Research, 2012 , vol. 36, # 9 p. 512 - 515
反应条件
1: 71 percent / NEt3 / CH2Cl2 / 6 h / Heating
2: 84 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 8 h / Heating
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参考文献
Chun; Park; Oh; Hong; Kim
Synthesis, 1994 , # 9 p. 909 - 910
参考文献
Abbott Laboratories
Patent: US6294573 B1, 2001 ;
US 6294573 B1
