136918-14-4合成路线 （共 708 条）
反应条件
sodium tetrahydroborate; potassium carbonate in dichloromethane; water
T=0 - 15°C;
参考文献
Rajan, Ramya; Badgujar, Sachin; Kaur, Kamaljit; Malpani, Yashwardhan; Kanjilal, Pranab R.
Synthetic Communications, 2010 , vol. 40, # 19 p. 2897 - 2907
反应条件
[Ni(1,2-bis(di-isopropylphosphino)ethane)(μ-H)]2; hydrogen in tetrahydrofuran
T=140°C; P=38787.1 Torr; 72 h; AutoclaveGlovebox;
参考文献
Arevalo, Alma; Ovando-Segovia, Sebastian; Flores-Alamo, Marcos; Garcia, Juventino J.
Organometallics, 2013 , vol. 32, # 10 p. 2939 - 2943
反应条件
sulfuric acid
T=40°C; Bei der elektrochemischen Reduktion an einer Zink-Amalgam-Kathode unter Normaldruck,bei 5.3 at und bei 8.5 at;
参考文献
Sakurai
Bl.Fac.lib.Arts Sci.Shinshu Univ., 1955 , # 5 p. Tl.2,S.11,14
反应条件
titanium tetrachloride; potassium carbonate; zinc
1.) 110 deg C, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Dunet; Willemart
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 222, p. 1443
反应条件
titanium tetrachloride; potassium carbonate; zinc
1.) xylene, 110 deg C, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Li, Jing; Chen, Jian; Chen, Hai-Bo; Chen, Wei-Xing
Synthetic Communications, 1998 , vol. 28, # 7 p. 1281 - 1286
反应条件
P=6251.8 Torr; Elektrochemische Reduktion an einer Zink-Amalgam-Kathode;
参考文献
Sakurai
Bulletin of the Chemical Society of Japan, 1932 , vol. 7, p. 155
参考文献
Graebe
Chemische Berichte, 1884 , vol. 17, p. 2598
Justus Liebigs Annalen der Chemie, 1888 , vol. 247, p. 291
反应条件
1.1: nitric acid; sulfuric acid / 16 h / 5 - 20 °C
2.1: potassium hydroxide / methanol; ethanol / 3 h / 20 °C
2.2: 1 h / |Reflux
View Scheme
参考文献
Bian, Xiaoli; Wang, Qian; Ke, Changhu; Zhao, Guilan; Li, Yiping
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 7 p. 2022 - 2026
参考文献
Bond; Luttermoser
Journal of the American Pharmaceutical Association (1912-1977), 1954 , vol. 43, p. 32,33
Full Text Show Details
Phillips; Pitt
Journal of the American Chemical Society, 1943 , vol. 65, p. 1355
反应条件
Aliquatreg; 336; potassium carbonate in N,N-dimethyl-formamide
20 h;
参考文献
Koc, Fikret; Eilbracht, Peter
Tetrahedron, 2004 , vol. 60, # 38 p. 8465 - 8476
