136918-14-4合成路线 （共 708 条）
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran
T=90°C; 7 h; Inert atmosphere; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
反应条件
triphenylphosphine; diethylazodicarboxylate
T=0 - 20°C; 18 h; Inert atmosphereSchlenk technique;
参考文献
Zheng, Xin; Cao, Bonan; Liu, Tang-Lin; Zhang, Xumu
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 679 - 684
反应条件
[Cu(μ-OH)(tmeda)]2Cl2; caesium carbonate in acetonitrile
T=20°C; 4 h;
参考文献
Kumaraswamy; Pitchaiah; Ramakrishna; Sadaiah
Tetrahedron Letters, 2006 , vol. 47, # 12 p. 2013 - 2015
反应条件
1: ethanol / 0.17 h / 50 °C
2: N,N-dimethyl-formamide / 0.25 h / 160 °C
View Scheme
参考文献
Bugaev; Dmitriev; Prosenko
Russian Chemical Bulletin, 2012 , vol. 61, # 2 p. 298 - 302
Izv. Akad. Nauk, Ser. Khim., 2012 , # 2 p. 297 - 301,5
反应条件
triethylamine in acetone
T=0°C; 0.25 h;
参考文献
Stephens; Domeier
Synthetic Communications, 1991 , vol. 21, # 20 p. 2025 - 2032
反应条件
potassium hydroxide
T=180°C; unter vermindertem Druck;
参考文献
Poppelsdorf; Holt
Journal of the Chemical Society, 1954 , p. 4094,4099
参考文献
Gabriel
Chemische Berichte, 1880 , vol. 13, p. 1684
Chemische Berichte, 1885 , vol. 18, p. 3478
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran
T=90°C; 5.5 h; Inert atmosphere; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
反应条件
triphenylphosphine; diethylazodicarboxylate
T=0 - 20°C;
参考文献
Sun, Xianfeng; Zhou, Le; Li, Wei; Zhang, Xumu
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 1143 - 1146
反应条件
1,3-bis-(diphenylphosphino)propane; sodium acetate; acetic acid in toluene
T=90°C;
参考文献
Trost, Barry M.; Dake, Gregory R.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5670 - 5671
