136918-14-4合成路线 （共 708 条）
反应条件
bis(3-(perfluoro-t-butyloxy)propyl)diazodicarboxylate; PPh2(p-C6H4-C2H4C8F17) in tetrahydrofuran
T=20°C; Mitsunobu reaction; Inert atmosphere;
参考文献
Chu, Qianli; Henry, Christopher; Curran, Dennis P.
Organic Letters, 2008 , vol. 10, # 12 p. 2453 - 2456
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 6 h;
参考文献
Xiong, Tao; Li, Yan; Mao, Lujia; Zhang, Qian
Chemical Communications, 2012 , vol. 48, # 16 p. 2246 - 2248
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate
4 h; Heating;
参考文献
Krompiec, Stanislaw; Pigulla, Mariola; Szczepankiewicz, Wojciech; Bieg, Tadeusz; Kuznik, Nikodem; Leszczynska-Sejda, Katarzyna; Kubicki, Maciej; Borowiak, Teresa
Tetrahedron Letters, 2001 , vol. 42, # 40 p. 7095 - 7098
反应条件
triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=100°C; 5 h;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Toyofuku, Masanori; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 3021 - 3022
反应条件
[(PPh3)3Pd] in N,N-dimethyl-formamide
T=100°C; 5 h; oth. temperature;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Toyofuku, Masanori; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 3021 - 3022
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran
T=90°C; 4 h; Inert atmosphere; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
反应条件
[(PPh3)3Pd] in N,N-dimethyl-formamide
5 h; Ambient temperature;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Toyofuku, Masanori; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 3021 - 3022
反应条件
in N,N-dimethyl-formamide
参考文献
Merck and Co., Inc.
Patent: US3989749 A1, 1976 ;
反应条件
triethylamine in N-methyl-acetamide; water
参考文献
Aziende Colori Nazionali Affini ACNA S.p.A.
Patent: US4011224 A1, 1977 ;
反应条件
pyridine in butan-1-ol
参考文献
Baxter, Ellen W.; Reitz, Allen B.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 7 p. 763 - 768
