136918-14-4合成路线 (共 708 条)
反应条件
pyridine; oxygen; copper diacetate in dichloromethane 168 h;
参考文献
Huegel, Helmut M.; Rix, Colin J.; Fleck, Karin
Synlett, 2006 , # 14 p. 2290 - 2292
反应条件
[bis(acetoxy)iodo]benzene T=140°C; 4 h; chemoselective reaction;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483
反应条件
dichloro bis(acetonitrile) palladium(II) in 1,2-dichloro-ethane T=80°C; 24 h;
参考文献
Liu, Guosheng; Stahl, Shannon S.
Journal of the American Chemical Society, 2006 , vol. 128, # 22 p. 7179 - 7181
反应条件
1: 71 percent / aq. ammonium chloride, magnesium / methanol / 4 h / Heating 2: 90 percent / thionyl chloride / CHCl3 / 30 h / Ambient temperature 3: 60 percent / AlCl3 / 24 h / Ambient temperature View Scheme
参考文献
Kreher, Richard P.; Hennige, Hans; Konrad, Michael; Uhrig, Juergen; Clemens, Andrea
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1991 , vol. 46, # 6 p. 809 - 828
反应条件
sodium carbonate T=200°C;
参考文献
Shirley; Zeitz
Journal of Organic Chemistry, 1953 , vol. 18, p. 1591
反应条件
2: aqueous NaOH View Scheme
参考文献
Feist; Schultz
Archiv der Pharmazie (Weinheim, Germany), 1934 , vol. 272, p. 785,790
反应条件
T=100°C; 4 h; Title compound not separated from byproducts;
参考文献
Riggio; Hopff; Hofmann; Waser
Helvetica Chimica Acta, 1980 , vol. 63, # 2 p. 488 - 497
反应条件
in not given in presence of K2CO3;;
参考文献
Sommer, L. H.; Rockett, J.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5130 - 5134
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Gmelin Handbook: Si: MVol.C, 4, page 14 - 18
反应条件
2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides in tetrahydrofuran T=60°C; 5 h;
参考文献
Drew; Kelly
Journal of the Chemical Society, 1941 , p. 637,639
参考文献
Pratt; Brill
Chem. Zentralbl., 1915 , vol. 86, # I p. 834