136918-14-4合成路线 （共 708 条）
反应条件
[bis(acetoxy)iodo]benzene T=145°C; 3 h; Microwave irradiation;
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
N-benzyl-N,N,N-trimethyl-ammonium chloride; sodium carbonate in isopropyl alcohol T=25°C; 22 h;
参考文献
DAISO CO., LTD.
Patent: EP1403267 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran 3 h; Inert atmosphereReflux; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
参考文献
Gelo; Sunjic
Synthesis, 1993 , # 9 p. 855 - 857
反应条件
tri-tert-butyl phosphine; [bis(acetoxy)iodo]benzene; palladium diacetate T=100°C; 33 h; Inert atmosphereGlovebox; Overall yield = 82 percent; Overall yield = 247 mg;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483
反应条件
[bis(acetoxy)iodo]benzene T=140°C; 4 h;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483
反应条件
1: water / 1 h / Reflux 2: nitric acid; acetic anhydride; urea / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Dos Santos, Jean Leandro; Lanaro, Carolina; Lima, Ldia Moreira; Gambero, Sheley; Franco-Penteado, Carla Fernanda; Alexandre-Moreira, Magna Suzana; Wade, Marlene; Yerigenahally, Shobha; Kutlar, Abdullah; Meiler, Steffen E.; Costa, Fernando Ferreira; Chung, Manchin
Journal of Medicinal Chemistry, 2011 , vol. 54, # 16 p. 5811 - 5819
反应条件
L-proline in neat (no solvent) T=130°C; 30 h; Sealed tube;
参考文献
Rao, Sadu Nageswara; Mohan, Darapaneni Chandra; Adimurthy, Subbarayappa
Organic Letters, 2013 , vol. 15, # 7 p. 1496 - 1499
反应条件
potassium carbonate; N,N-dimethyl-formamide; potassium iodide T=140°C;
参考文献
Billmann; Cash
Proceedings of the Indiana Academy of Science, 1952 , vol. 62, p. 158
反应条件
T=-20°C; Addition; solid-gas reaction; ring cleavage; P=75.006 Torr;
参考文献
Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen
Tetrahedron, 2000 , vol. 56, # 36 p. 6899 - 6911
