in chloroform-d1 0.233333 h; Irradiation;

<b>Multi-step reaction with 8 steps<br /> </b>1: phosphorous pentoxide; phosphoric acid / 3.25 h / 70 &deg;C / Inert atmosphere<br />2: ammonium cerium (IV) nitrate; iodine / acetonitrile / 60 &deg;C / Inert atmosphere<br />3: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; N,N-dimethyl-formamide / 4 h / 80 &deg;C / Inert atmosphere<br />4: selenium(IV) oxide / 1,2-dichloro-benzene / 150 &deg;C / Inert atmosphere<br />5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 &deg;C / Inert atmosphere<br />6: ethanol / 24 h / 20 &deg;C / Inert atmosphere<br />7: sodium hydroxide / dichloromethane; water / 20 &deg;C / Inert atmosphere<br />8: hydrogenchloride / chloroform; water / 6 h / 60 &deg;C / pH 4 / Inert atmosphere<br /> <br /> &nbsp;