Craig; Robinson; Fowler
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1610
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Robinson et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1596,1598
(Et4N)(ClO4) in acetone
Electrolysis; under flush of Ar; electrolytic oxidn. of the metal in a glass cell in the presence of an acetone soln. of the thiuram disulphide ((NEt4)(ClO4)as electrolyte), current flow at 50 V, 50 min; solvent is reduced in vac., petroleum ether is added, compd. is dried in vac.;
参考文献
Casey, Allan T.; Vecchio, Angelica M.
Inorganica Chimica Acta, 1987 , vol. 131, p. 191 - 194
