(±)-2-甲基-1-丁醇合成路线 （共 128 条）
反应条件
1: 67.7 percent / methyl iodide, triphenyl phosphite / 20 h / Heating 2: 49.8 percent / benzene / 20 h / Heating 3: 1.) BuLi / 1.) ether, hexane, 30 min, 2.) ether, hexane, 1 h 4: H2 / 5percent Pd/C / ethanol View Scheme
参考文献
Suzuki, Takahisa
Agricultural and Biological Chemistry, 1981 , vol. 45, # 6 p. 1357 - 1364
参考文献
Evers et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 1138
反应条件
triphenyl phosphite; methyl iodide 20 h; Heating;
参考文献
Suzuki, Takahisa
Agricultural and Biological Chemistry, 1981 , vol. 45, # 6 p. 1357 - 1364
参考文献
Berlak; Gerrard
Journal of the Chemical Society, 1949 , p. 2310
反应条件
bromine; triphenylphosphine in N,N-dimethyl-formamide Title compound not separated from byproducts;
参考文献
Suzuki, Takahisa; Ozaki, Jotaro; Sugawara, Ryozo
Agricultural and Biological Chemistry, 1983 , vol. 47, # 4 p. 869 - 876
参考文献
Mistry,N.N.; Thaker,K.A.
Journal of the Indian Chemical Society, 1969 , vol. 46, p. 995 - 996
反应条件
sodium lauryl sulfate; sodium hydroxide; palladium dichloride; (4-dimethylaminophenyl)-diphenylphosphine in water T=44.84°C; P=760 Torr; Inert atmosphere; Kinetics;
参考文献
Norman, Carnley; Wilhite, Benjamin A.; Pham, Due; Lim, Phooi K.; Brown, Philip A.
Organic Process Research and Development, 1998 , vol. 2, # 6 p. 366 - 378
反应条件
sodium lauryl sulfate; sodium hydroxide; palladium dichloride; (4-dimethylaminophenyl)-diphenylphosphine in water T=44.84°C; P=760 Torr; Inert atmosphere; Kinetics;
参考文献
Norman, Carnley; Wilhite, Benjamin A.; Pham, Due; Lim, Phooi K.; Brown, Philip A.
Organic Process Research and Development, 1998 , vol. 2, # 6 p. 366 - 378
参考文献
Lieben; Zeisel
Monatshefte fuer Chemie, 1886 , vol. 7, p. 68
参考文献
Ssuknewitsch; Tschilingarjan
Chemische Berichte, 1935 , vol. 68, p. 1211,1216
Chemische Berichte, 1936 , vol. 69, p. 1538,1539,1541,1542
