(±)-2-甲基-1-丁醇合成路线 （共 128 条）
反应条件
aluminum oxide T=380 - 400°C;
参考文献
Evers et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 1138
反应条件
1.1: pyridine / 3 h / 0 - 5 °C 2.1: lithium bromide / N,N-dimethyl-formamide / 1 h / 60 °C 3.1: magnesium / tetrahydrofuran / Inert atmosphere 3.2: -70 - 20 °C / Inert atmosphere View Scheme
参考文献
Mori, Kenji
Bioscience, Biotechnology and Biochemistry, 2010 , vol. 74, # 3 p. 595 - 600
反应条件
N-bromosuccinmide; L-proline in water T=20°C; 3 h;
参考文献
Liu, Xiuhong; Wu, Jun; Shang, Zhicai
Synthetic Communications, 2012 , vol. 42, # 1 p. 75 - 83
反应条件
D-glucose; Gluconobacter oxidans DSM 2343; yeast extract in phosphate buffer T=28°C; pH=6.3; 6 h; Enzymatic reaction;
参考文献
Tetrahedron Letters, , vol. 43, # 34 p. 6059 - 6061
反应条件
(4,5-bis-(di-iso-propylphosphinomethyl)acridine)RuH(CO)Cl; ammonia in toluene P=5700.38 Torr; 18 h; Inert atmosphereReflux;
参考文献
Gunanathan, Chidambaram; Milstein, David
Angewandte Chemie - International Edition, 2008 , vol. 47, # 45 p. 8661 - 8664
反应条件
aluminium hydroxide hydrate; ammonia T=400°C; P=147102 Torr;
参考文献
I.G. Farbenind.
Patent: FR747905 , 1933 ;
Full Text Show Details
I.G. Farbenind.
Patent: US2082105 , 1932 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE631737 , 1931 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 23, p. 174
反应条件
4-(N,N-dimethlyamino)pyridine
参考文献
Strobel, Gary A.; Manker, Denise Carol; Mercier, Julien; Jimenez, Jorge; Lin, John; Thurston, Jonathan; Kersting, Barry
Patent: US2004/141955 A1, 2004 ;
反应条件
sodium hydrogen sulphate; silica gel 1 h; Heating;
参考文献
Nishiguchi, Takeshi; Taya, Hisachi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 172 - 173
参考文献
Sarel; Newman
Journal of the American Chemical Society, 1956 , vol. 78, p. 5416,5418
反应条件
sodium hydride 1.) 2 h, reflux, 2.) 1 h, reflux; Multistep reaction;
参考文献
Cohen, Yael; Afri, Michal; Frimer, Aryeh A.
Chemistry and Physics of Lipids, 2008 , vol. 155, # 2 p. 120 - 125
