(±)-2-甲基-1-丁醇合成路线 (共 128 条)
反应条件
Na2S2O5; Origanum dayi alcohol acetyl transferase in glycerol T=30°C; pH=7.5; 0.5 h; Enzymatic reaction; Reactivity; Reagent/catalyst;
参考文献
Larkov, Olga; Zaks, Alon; Bar, Einat; Lewinsohn, Efraim; Dudai, Nativ; Mayer, Alfred M.; Ravid, Uzi
Phytochemistry, 2008 , vol. 69, # 14 p. 2565 - 2571
反应条件
sulfuric acid; dihydrogen peroxide; sodium tungstate in water; acetonitrile T=80°C; 6 h;
参考文献
Bhati, Nishi; Sarma, Kuladip; Goswami, Amrit
Synthetic Communications, 2008 , vol. 38, # 9 p. 1416 - 1424
反应条件
1.1: pyridine / 3 h / 0 - 5 °C 2.1: lithium bromide / N,N-dimethyl-formamide / 1 h / 60 °C 3.1: magnesium / diethyl ether 3.2: -70 - 20 °C View Scheme
参考文献
Mori, Kenji
Bioscience, Biotechnology and Biochemistry, 2010 , vol. 74, # 3 p. 595 - 600
反应条件
sulfuric acid; hydrogen bromide; sodium carbonate in water
参考文献
Kao Corporation
Patent: US5476649 A1, 1995 ;
参考文献
Evers et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 1138
反应条件
sulfuric acid; dihydrogen peroxide; sodium tungstate in water; acetonitrile T=80°C; 6 h;
参考文献
Synthetic Communications, , vol. 38, # 9 p. 1416 - 1424
参考文献
Streitwieser et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 1110
反应条件
zinc(II) chloride T=165 - 170°C;
参考文献
Abbott Labor.
Patent: US2073995 , 1934 ;
Full Text Show Details
Abbott Labor.
Patent: US2106760 , 1934 ;
反应条件
1: With (R,R,R,R)-(-)-trans,trans-2,3,10,11-tetrakis(hydroxydiphe.. T=20°C; inclusion complexation; resolution of racemate; 24 h; 2: T=180°C; decomposition of complex; P=30 Torr;
参考文献
Tanaka, Koichi; Honke, Shinji; Urbanczyk-Lipkowska, Zofia; Toda, Fumio
European Journal of Organic Chemistry, 2000 , # 18 p. 3171 - 3176
反应条件
vinyl acetate; pseudomonas fluorescens lipase in dichloromethane Enzymatic reaction;
参考文献
McAllister, Graeme D.; Taylor, Richard J. K.
Tetrahedron Letters, 2004 , vol. 45, # 12 p. 2551 - 2554