1: With borane-THF in tetrahydrofuran T=20°C; 2 h; 2: With sodium hydroxide; dihydrogen peroxide in diethyl ether 0.5 h; 3: With phosphorus tribromide in pentane 12 h; Heating; Title compound not separated from byproducts;
N-bromosuccinmide; bromine in dichloromethane; cyclohexane T=15°C; Irradiationrelative reactivity; other cycloalkanes; other bromination agents; var temp.; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 50, # 9 p. 1534 - 1538
N-bromosuccinmide; cyclohexane in acetonitrile T=23°C; 16 h; IrradiationEffect of solvent on the Relative Rates of Bromination; Effect of Added Bromine; Effect of Added Olefine (C2H4); Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 48, # 16 p. 2743 - 2747
