反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '106420', constants.ctx, '0')">1-methyl-pyrrolidin-2-one</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a>; <a href="#" onclick="return RXDsubstances(event, this, '605284', constants.ctx, '0')">diisopropylamine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=-78°C; 0.25 h; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '509751', constants.ctx, '0')">benzyl chloroformate</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=-78°C; 1 h; Inert atmosphere; <br /> <br />
参考文献
Moody, Catherine L.; Franckevicius, Vilius; Drouhin, Pauline; Klein, Johannes E.M.N.; Taylor, Richard J.K. Tetrahedron Letters, 2012 , vol. 53, # 15 p. 1897 - 1899