1,1,2,2-四氯-二硼烷合成路线 （共 63 条）
反应条件
stable HBCl2/BCl3 mixt. obtained after fracti onation of react. mixt. in cold traps, HBCl2/BCl3 mixt. trapped at -112°C;
参考文献
Kotz; Post
Inorganic Chemistry, 1970 , vol. 9, p. 1661,1664
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Gmelin Handbook: B: B-Verb.9, 1.2.2.1, page 15 - 20
参考文献
Gmelin Handbook: B: B-Verb.9, 1.2.2.1, page 15 - 20
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Barr, J. B.
Diss. Abstr., Thesis Pennsylvania State Univ. 1961 1961 , vol. 22, p. 86/7
反应条件
26°C; 30 Torr; IR anal. suggests that the unstable intermediate enriched in -150 - -130°C fraction is probably unsymmetric B2H4Cl2;
参考文献
Rietti, S. B.; Lombardo J.
Journal of Inorganic and Nuclear Chemistry, 1965 , vol. 27, p. 247 - 249
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Gmelin Handbook: B: B-Verb.9, 2.2, page 54 - 55
反应条件
room temp.; B2H5Cl detected by IR spectroscopy after 22.5 h;
参考文献
Gmelin Handbook: B: B-Verb.9, 1.2.2.1, page 15 - 20
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Barr, J. B.
Diss. Abstr., Thesis Pennsylvania State Univ. 1961 1961 , vol. 22, p. 86/7
反应条件
compn. of gas phase final product studied by IR spectroscopy;
参考文献
Gmelin Handbook: B: B-Verb.9, 2.1.2.1, page 45 - 47
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Barr, J. B.
Diss. Abstr., Thesis Pennsylvania State Univ. 1961 1961 , vol. 22, p. 86/7
反应条件
byproducts: BCl3, CH3BCl2; excess of B2Cl4, violent react. at -78°C, then decompn. at 20.fegree.C;
参考文献
Gmelin Handbook: B: B-Verb.4, 4.9.3, page 181 - 204
参考文献
Gmelin Handbook: B: B-Verb.9, 4.2.5, page 131 - 132
反应条件
excess of (CH3)2BN(CH3);
参考文献
Gmelin Handbook: B: B-Verb.4, 4.9.3, page 181 - 204
参考文献
Gmelin Handbook: B: B-Verb.9, 5.2.8.2, page 220 - 226
参考文献
Ritter,J.J. et al.
Journal of Organometallic Chemistry, 1971 , vol. 29, p. 175 - 184
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Gmelin Handbook: B: B-Verb.9, 5.2.2, page 173 - 181
