1: acetonitrile / 1 h 2: NaBH3CN / acetonitrile / 12 h / 50 °C 3: 85 percent / molecular sieves 3 Angstroem / ethanol / 72 h / Heating 4: hydrogen, 60percent HClO4 / Pd-black / acetic acid / 20 h / Ambient temperature 5: 5 M KOH / methanol / 3 h / Ambient temperature 6: DCC / tetrahydrofuran 7: BH3*SMe2 / tetrahydrofuran / 3 h / Ambient temperature 8: CAN / acetonitrile; H2O / 0.08 h / Ambient temperature 9: 74 percent / Na2CO3 / ethanol / 3 h / Ambient temperature 10: 24 percent / LiClO4 / acetonitrile / 1 h / electrolysis View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587189', constants.ctx, '0')">hydrogen</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '11378922', constants.ctx, '0')">palladium on activated charcoal</a> <br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: toluene / 2 h / 60 &deg;C<br />2: 100 percent / hydrogen / 10percent Pd-C / ethanol / 2 h<br /> <br /> &nbsp;