palladium 10 on activated carbon; hydrogen in methanol 72 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098214', constants.ctx, '0')">hydrogenchloride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209237', constants.ctx, '0')">ethylene glycol dimethyl ether</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />4&nbsp;h;&nbsp;&nbsp;Reflux;&nbsp;<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: iodine; magnesium / tetrahydrofuran / Inert atmosphere; Reflux<br />1.2: 3 h / 20 &deg;C / Inert atmosphere; Cooling with ice<br />2.1: hydrogenchloride / ethylene glycol dimethyl ether; water / 4 h / Reflux<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: iodine; magnesium / tetrahydrofuran / Inert atmosphere; Reflux<br />1.2: 3 h / 20 &deg;C / Inert atmosphere; Cooling with ice<br />2.1: hydrogenchloride / ethylene glycol dimethyl ether; water / 4 h / Reflux<br /> <br /> &nbsp;