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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1370331-08-0
合成路线
(共 3 条)
1370331-08-0
→
反应条件
531-95-3
雌马酚
反应条件
1: With triethylsilane; boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; 15.5 h; 2: With hydrogen; palladium(II) oxide hydrate; acetic acid in tetrahydrofuran; ethyl acetate P=7600.51 Torr; 36 h;
参考文献
Tilley, Andrew J.; Zanatta, Shannon D.; Qin, Cheng Xue; Kim, In-Kyeom; Seok, Young-Mi; Stewart, Alastair; Woodman, Owen L.; Williams, Spencer J.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2353 - 2361
1370331-08-0
→
反应条件
531-95-3
雌马酚
反应条件
1: With triethylsilane; boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; 15.5 h; 2: With hydrogen; palladium(II) oxide hydrate; acetic acid in tetrahydrofuran; ethyl acetate P=7600.51 Torr; 36 h;
参考文献
Tilley, Andrew J.; Zanatta, Shannon D.; Qin, Cheng Xue; Kim, In-Kyeom; Seok, Young-Mi; Stewart, Alastair; Woodman, Owen L.; Williams, Spencer J.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2353 - 2361
1370331-08-0
→
反应条件
531-95-3
雌马酚
反应条件
1: With triethylsilane; boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; 15.5 h; 2: With hydrogen; palladium(II) oxide hydrate; acetic acid in tetrahydrofuran; ethyl acetate P=7600.51 Torr; 36 h;
参考文献
Tilley, Andrew J.; Zanatta, Shannon D.; Qin, Cheng Xue; Kim, In-Kyeom; Seok, Young-Mi; Stewart, Alastair; Woodman, Owen L.; Williams, Spencer J.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2353 - 2361