lithium aluminium tetrahydride in diethyl ether T=0 - 20°C; 3 h; Inert atmosphere;

1: With boron trifluoride diethyl etherate T=0°C; 3 h; 2: With lithium aluminium tetrahydride in diethyl ether T=0 - 20°C; 3 h;

1: boron trifluoride diethyl etherate / 3 h / 0 °C / Inert atmosphere; Neat (no solvent) 2: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere View Scheme