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乙二醇
甲醛
63148-62-9
MDI
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1370649-95-8
合成路线
（共 5 条）
1370649-95-8
→
反应条件
830-13-7
环十二酮
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 2.1: methanol; water; sodium hydroxide / 5 h / Reflux 2.2: 1 h / Reflux 3.1: iodine; potassium hydroxide / -5 - 0 °C 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 5.1: methanol; water; sodium hydroxide / 5 h / Reflux 5.2: 1 h / Reflux View Scheme
参考文献
Helvetica Chimica Acta, , vol. 95, # 3 p. 428 - 447
1370649-95-8
→
反应条件
832-10-0
环三癸酮
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 2.1: methanol; water; sodium hydroxide / 5 h / Reflux 2.2: 1 h / Reflux View Scheme
参考文献
Chapuis, Christian; Robvieux, Fabrice; Cantatore, Carole; Saint-Leger, Christine; Maggi, Laurent
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 428 - 447
1370649-95-8
→
反应条件
878-13-7
环十一酮
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 2.1: methanol; water; sodium hydroxide / 5 h / Reflux 2.2: 1 h / Reflux 3.1: iodine; potassium hydroxide / -5 - 0 °C 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 5.1: methanol; water; sodium hydroxide / 5 h / Reflux 5.2: 1 h / Reflux 6.1: iodine; potassium hydroxide / -5 - 0 °C 7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 8.1: methanol; water; sodium hydroxide / 5 h / Reflux 8.2: 1 h / Reflux View Scheme
参考文献
Chapuis, Christian; Robvieux, Fabrice; Cantatore, Carole; Saint-Leger, Christine; Maggi, Laurent
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 428 - 447
1370649-95-8
→
反应条件
33059-17-5
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 2.1: methanol; water; sodium hydroxide / 5 h / Reflux 2.2: 1 h / Reflux 3.1: iodine; potassium hydroxide / -5 - 0 °C 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 5.1: methanol; water; sodium hydroxide / 5 h / Reflux 5.2: 1 h / Reflux 6.1: potassium tert-butylate / tert-butyl alcohol / 50 °C View Scheme
参考文献
Chapuis, Christian; Robvieux, Fabrice; Cantatore, Carole; Saint-Leger, Christine; Maggi, Laurent
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 428 - 447
1370649-95-8
→
反应条件
1502-06-3
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 2.1: methanol; water; sodium hydroxide / 5 h / Reflux 2.2: 1 h / Reflux 3.1: iodine; potassium hydroxide / -5 - 0 °C 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 5.1: methanol; water; sodium hydroxide / 5 h / Reflux 5.2: 1 h / Reflux 6.1: iodine; potassium hydroxide / -5 - 0 °C 7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 8.1: methanol; water; sodium hydroxide / 5 h / Reflux 8.2: 1 h / Reflux 9.1: iodine; potassium hydroxide / -5 - 0 °C 10.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C 11.1: methanol; water; sodium hydroxide / 5 h / Reflux 11.2: 1 h / Reflux View Scheme
参考文献
Chapuis, Christian; Robvieux, Fabrice; Cantatore, Carole; Saint-Leger, Christine; Maggi, Laurent
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 428 - 447
