1,4,7,10-四氮杂环十二烷-1,4,7,10-四乙酸三叔丁酯合成路线 (共 19 条)
反应条件
sodium hydroxide in water T=50°C;
参考文献
Tetrahedron Letters, , vol. 50, # 24 p. 2929 - 2931
反应条件
1: sodium carbonate / acetonitrile / 24 h / 70 °C 2: sodium hydroxide / methanol; water / 24 h / 20 °C View Scheme
参考文献
Inorganic Chemistry, , vol. 51, # 19 p. 10366 - 10374
反应条件
1: potassium carbonate / acetonitrile / 16 h / 20 °C 2: tetrakis(triphenylphosphine) palladium(0); 4-methyl-morpholine / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 50 p. 6810 - 6814
反应条件
1: sodium hydrogencarbonate / acetonitrile / 40 h / 20 °C 2: potassium carbonate / acetonitrile / 60 °C 3: palladium 10 on activated carbon; hydrogen / methanol / 6 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7410 - 7413
反应条件
1: |Alkaline conditions 2: potassium carbonate / acetonitrile 3: palladium on activated charcoal; hydrogen / methanol View Scheme
参考文献
Amino Acids, , vol. 46, # 2 p. 449 - 457
参考文献
Oliver, Morag; Jorgensen, Michael R.; Miller, Andrew D.
Synlett, 2004 , # 3 p. 453 - 456
反应条件
tri-iso-propylsilane; water; trifluoroacetic acid 3 h; TimeReagent/catalystSolvent;
参考文献
Tetrahedron Letters, , vol. 53, # 50 p. 6810 - 6814
反应条件
tri-iso-propylsilane; water; trifluoroacetic acid 3 h; TimeReagent/catalystSolvent;
参考文献
Tetrahedron Letters, , vol. 53, # 50 p. 6810 - 6814
反应条件
1: N-hydroxysuccinimide; HBTU / dimethylformamide / 24 h / 20 °C
2: aq. tris(2-carboxyethyl)phosphine hydrochloride / dioxane / pH 7
3: 0.2 g / aq. TFA; triisopropylsilane / 20 h
View Scheme
参考文献
Mattila, Kati; Siltainsuu, Jaana; Balaspiri, Lajos; Ora, Mikko; Loennberg, Harri
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 16 p. 3039 - 3044