2-(吲哚-1-基)乙胺合成路线 (共 15 条)
反应条件
lithium aluminium tetrahydride in diethyl ether 2.5 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 31, # 3 p. 284 - 288
Khimiya Geterotsiklicheskikh Soedinenii, , # 3 p. 331 - 335
反应条件
Raney nickel in tetrahydrofuran 5 h; Reflux;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 46, # 3 p. 291 - 301
反应条件
sodium methylate; potassium iodide in methanol T=15°C; Electrochemical reaction;
参考文献
Australian Journal of Chemistry, , vol. 60, # 4 p. 236 - 242
反应条件
1: 20 percent / KI; NaOMe / methanol / 15 °C / Electrochemical reaction View Scheme
参考文献
Australian Journal of Chemistry, , vol. 60, # 4 p. 236 - 242
反应条件
1: tetrabutyl-ammonium chloride; sodium hydroxide / dichloromethane / 10 h / Reflux 2: sodium azide / N,N-dimethyl-formamide / 3 h / 80 °C 3: water; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 14, # 3 p. 844 - 847
反应条件
1: 34 g / 10percent Pd-C / xylene / 1.5 h / Heating 2: 18 g / KOH / ethanol; H2O / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 3 p. 900 - 909
反应条件
1: sodium azide / N,N-dimethyl-formamide / 3 h / 80 °C 2: water; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 14, # 3 p. 844 - 847
反应条件
potassium hydroxide in ethanol; water Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 3 p. 900 - 909
反应条件
sodium hydroxide in acetonitrile
参考文献
Tetrahedron, , vol. 61, # 40 p. 9513 - 9518
反应条件
1.1: 3-chloro-benzenecarboperoxoic acid 2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 25 °C 2.2: 10 h / 25 °C 3.1: Raney nickel / tetrahydrofuran / 5 h / Reflux View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 46, # 3 p. 291 - 301