Gmelin Handbook: Sc: MVol.C3, 6.2.5.2.1.1, page 147 - 148
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Carlson, O. N.; Schmidt, F. A.; Spedding, F. H.
C. A., ISC-744 (1956) 1/22 1957 , p. 921
in neat (no solvent) at room temp. in presence of moisture;;
参考文献
Popov, A. I.; Knudson, E. G.
Journal of the American Chemical Society, 1954 , vol. 76, p. 3921 - 3922
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Gmelin Handbook: Sc: MVol.C3, 6.2.2.1.8, page 38 - 38
sodium linoleate; linoleic acid in ethanol; water High Pressure; Na linoleate, linoleic acid and EtOH mixed under agitation; aq. soln. ofY(NO3)3 and NH4HF2 added; agitated for ca. 5 min; transefrred to autocl ave; sealed; hydrothermally treated at 100-200°C for 8-10 h; cooled to room temp.; deposit dispersed in cyclohexane; EtOH added; centrifuged; powder purified with EtOH several times; detd. by X-ray powder diffraction and electron microscopy; YF3 nanocrystals obtained;
sodium linoleate; linoleic acid in ethanol; water High Pressure; Na linoleate, linoleic acid and EtOH mixed under agitation; aq. soln. ofY(NO3)3 and NaF added; agitated for ca. 5 min; transefrred to autoclave ; sealed; hydrothermally treated at 100-200°C for 8-10 h; cooled to room temp.; deposit dispersed in cyclohexane; EtOH added; centrifuged; powder purified with EtOH several times; detd. by X-ray powder diffraction and electron microscopy; YF3 and NaYF4 nanocrystals obtained;
HCl in water; ethylenediamine High Pressure; ethylenediamine and NH4F were added with stirring to aq. soln. of Y(NO3)3; HCl was added to pH 1-7; agitated for 30 min; heated in autoclave at 180°C for 12 h; cooled to room temp.; collected; washed (EtOH, H2O); dried at 80°C for 12 h; calcined at 600°C for 4 h;
trisodium citrate dihydrate in water High Pressure; under hydrothermal conditions; Y2O3 dissolved in HCl at elevated temp.; added to aq. soln. of C6H5O7Na3*2H2O; stirred (30 min); aq. NaBF4 added;pH adjusted to 1 (aq. HCl); agitated (15 min); heated in autoclave (180 °C, 24 h); cooled to room temp. naturally; ppt. sepd by centrifugation; washed withEtOH and deionized H2O; dried in air at 80°C for 12 h; detd. by X-ray diffraction; YF3 microspindles obtained;
