反应条件
n-butyllithium in tetrahydrofuran under Ar or N2, Schlenk technique; soln. of n-BuLi (1 equiv.) added dropwise to soln. of Fe compd. at -60°C, mixt. stirred at room temp. for 0.5 h, cooled to -30°C, P compd. (1 equiv.) added dropwise, mixt. stirred at room temp. for 1 h; concn. under vac., chromy. (n-hexane), dried under vac.;
参考文献
Milde, Bianca; Lohan, Manja; Schreiner, Claus; Rueffer, Tobias; Lang, Heinrich
European Journal of Inorganic Chemistry, 2011 , # 35 p. 5437 - 5449
