反应条件
in toluene under N2, toluene soln. of phosphine was added to toluene soln. of Pd-complex, after 1 h Br-compd. was added (molar ratio phosphine:Pd-complex:Br-compd. was 4:2:1), mixt. was stirred for 5 h; mixt. was filtered, soln. vol. was reduced to a half, equal amt. of acetone was added, soln. was left overnight at 4°C, elem. anal.;
参考文献
Vilar, Ramon; Mingos, D. Michael P.; Cardin, Christine J.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 23 p. 4313 - 4314
