二乙基三甲基硅基亚磷酸酯合成路线 （共 88 条）
反应条件
T=20°C; Substitution; 4 h;
参考文献
Saakyan
Russian Journal of General Chemistry, 1999 , vol. 69, # 11 p. 1712 - 1716
参考文献
Kamalov, R. M.; Stepanov, G. S.; Pudovik, M. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 2.2 p. 476 - 477,414 - 415
反应条件
in benzene 3 h; Heating;
参考文献
Sekine, Mitsuo; Nakajima, Masashi; Hata, Tsujiaki
Journal of Organic Chemistry, 1981 , vol. 46, # 20 p. 4030 - 4034
反应条件
T=150°C; 2 h; Mechanism;
参考文献
Sekine, Mitsuo; Nakajima, Masashi; Hata, Tsujiaki
Journal of Organic Chemistry, 1981 , vol. 46, # 20 p. 4030 - 4034
反应条件
T=80 - 100°C; P=50 Torr; 3 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 4 p. 769 - 776,667 - 673
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-10 - 25°C;
参考文献
Ku, Bonchul; Oh, Dong Young
Tetrahedron Letters, 1988 , vol. 29, # 35 p. 4465 - 4466
参考文献
Creary, Xavier; Geiger, Cristina C.; Hilton, Kathryn
Journal of the American Chemical Society, 1983 , vol. 105, # 9 p. 2851 - 2858
反应条件
1: 72 percent / benzene / 6 h / Ambient temperature 2: 1.) LDA / 1.) THF, hexane, -78 deg C, 5 h, 2.) THF, hexane, -78 deg C to RT, 1.5 h View Scheme
参考文献
Sekine, Mitsuo; Nakajima, Masashi; Kume, Akiko; Hashizume, Akio; Hata, Tsujiaki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 1 p. 224 - 238
参考文献
Novikova,Z.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 2622 - 2628,2655 - 2660
反应条件
T=20°C; Substitution; 4 h;
参考文献
Saakyan
Russian Journal of General Chemistry, 1999 , vol. 69, # 11 p. 1712 - 1716
