叔丁氧羰基-L-谷氨酸-5-叔丁酯合成路线 （共 8 条）
反应条件
1: 90 percent / NaOCH3 / methanol 2: NaBH4 / ethanol / 24 h / 20 °C 3: 80 percent / NaIO4 / H2O / 4 °C 4: acetonitrile 5: H2 / PtO2 6: NaIO4, RuO2 View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 9 p. 1253 - 1256
反应条件
1: acetonitrile 2: H2 / PtO2 3: NaIO4, RuO2 View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 9 p. 1253 - 1256
反应条件
1: 80 percent / NaIO4 / H2O / 4 °C 2: acetonitrile 3: H2 / PtO2 4: NaIO4, RuO2 View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 9 p. 1253 - 1256
反应条件
1: H2 / PtO2 2: NaIO4, RuO2 View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 9 p. 1253 - 1256
反应条件
ruthenium(IV) oxide; sodium periodate Yield given;
参考文献
Tetrahedron Letters, , vol. 31, # 9 p. 1253 - 1256
反应条件
1: 4-(N,N-dimethlyamino)pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h 2: 1 h 3: sodium carbonate / 1,4-dioxane; water / 10 - 20 °C 4: 1,4-dioxane; water / 16 h / 20 °C View Scheme
参考文献
Agnihotri, Geetanjali; Ukani, Rehman; Malladi, Subbalakshmi S.; Warshakoon, Hemamali J.; Balakrishna, Rajalakshmi; Wang, Xinkun; David, Sunil A.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 5 p. 1490 - 1510
反应条件
triethylsilane; trifluoroacetic acid in dichloromethane 1.08333 h; Ambient temperature;
参考文献
Mehta, Anita; Jaouhari, Rabih; Benson, Timothy J.; Douglas, Kenneth T.
Tetrahedron Letters, 1992 , vol. 33, # 37 p. 5441 - 5444
反应条件
1: 4-(N,N-dimethlyamino)pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h 2: 1 h 3: sodium carbonate / 1,4-dioxane; water / 10 - 20 °C View Scheme
参考文献
Agnihotri, Geetanjali; Ukani, Rehman; Malladi, Subbalakshmi S.; Warshakoon, Hemamali J.; Balakrishna, Rajalakshmi; Wang, Xinkun; David, Sunil A.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 5 p. 1490 - 1510
