2,3-萘磺酸二甲基乙酸酯合成路线 （共 20 条）
反应条件
Yield given. Multistep reaction;
参考文献
Synlett, , # 12 p. 1381 - 1383
参考文献
Journal of the Chemical Society, , p. 1739
参考文献
Morkved, Eva H.; Lakshmikantham; Cava, Michael P.
Tetrahedron Letters, 1996 , vol. 37, # 51 p. 9149 - 9150
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
US5298622 A1, ;
US 5298622 A
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Wu, An-Tai; Liu, Wen-Dar; Chung, Wen-Sheng
Journal of the Chinese Chemical Society, 2002 , vol. 49, # 1 p. 77 - 82
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Regents of the University of Minnesota
Patent: US5298622 A1, 1994 ;
US 5298622 A
反应条件
1: 96 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 0 °C
2: 70 percent / PPh3Br2 / CH2Cl2 / 10 h / 20 °C
3: 63 percent / sodium formaldehyde sulfoxylate; TBAB / dimethylformamide / 3 h / 20 °C
4: 54 percent / toluene / 4 h / 180 °C
View Scheme
参考文献
Wu, An-Tai; Liu, Wen-Dar; Chung, Wen-Sheng
Journal of the Chinese Chemical Society, 2002 , vol. 49, # 1 p. 77 - 82
参考文献
Buckle,D.R. et al.
Journal of Medicinal Chemistry, 1977 , vol. 20, p. 265 - 269
反应条件
1: (i) NaH, (ii) aq. HCl
2: H2O
View Scheme
参考文献
Jones,D.W.; Wife,R.L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 2722 - 2727
反应条件
1: 96 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 0 °C
2: 70 percent / PPh3Br2 / CH2Cl2 / 10 h / 20 °C
View Scheme
参考文献
Ohkawa; DiGiacomo; Larson; Takemori; Portoghese
Journal of Medicinal Chemistry, 1997 , vol. 40, # 11 p. 1720 - 1725
