2,5-二甲基苯甲酸甲酯合成路线 （共 14 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Deshpande, Girish Nilkanth; Weipert, Paul David; Ensley, Michael W.
Patent: US2011/251395 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
Fe(ClO4)3*xH2O; dihydrogen peroxide in water T=0 - 20°C; 20 h;
参考文献
Wu, Xiao-Feng; Darcel, Christophe
European Journal of Organic Chemistry, 2009 , # 8 p. 1144 - 1147
反应条件
sulfuric acid 48 h; Heating;
参考文献
Neudeck
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 185 - 200
反应条件
1: SOCl2 / 6 h / Heating 2: Ambient temperature View Scheme
参考文献
Ngola, Sarah M.; Kearney, Patrick C.; Mecozzi, Sandro; Russell, Keith; Dougherty, Dennis A.
Journal of the American Chemical Society, 1999 , vol. 121, # 6 p. 1192 - 1201
反应条件
Ambient temperature; Yield given;
参考文献
Maeda, Ryo; Wada, Takehiko; Mori, Tadashi; Kono, Shigeyuki; Kanomata, Nobuhiro; Inoue, Yoshihisa
Journal of the American Chemical Society, 2011 , vol. 133, # 27 p. 10379 - 10381
反应条件
in methanol T=65°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Gokhale, Abha; Schiess, Peter
Helvetica Chimica Acta, 1998 , vol. 81, # 2 p. 251 - 267
反应条件
titanium; silicon 0.75 h; Microwave irradiation;
参考文献
De la Hoz; Diaz-Ortiz; Fraile; Gomez; Mayoral; Moreno; Saiz; Vazquez
Synlett, 2001 , # 6 p. 753 - 756
反应条件
1: 90 percent / Friedel-Crafts alkylation 2: 84 percent / haloform reaction 3: 93.1 percent / conc. H2SO4 / 48 h / Heating View Scheme
参考文献
Neudeck
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 185 - 200
反应条件
1: 84 percent / haloform reaction 2: 93.1 percent / conc. H2SO4 / 48 h / Heating View Scheme
参考文献
Neudeck
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 185 - 200
反应条件
1: 40 percent / HBr / diazotization 2: 1.) Mg / 1.) ether, 2.) ether, reflux, 2 h; room temp., overnight View Scheme
参考文献
Neudeck
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 185 - 200
