N-alpha-叔丁氧羰基-L-赖氨酸合成路线 (共 44 条)
反应条件
ammonium formate; palladium on activated charcoal in methanol 0.0833333 h; Ambient temperature;
参考文献
Channe Gowda
Tetrahedron Letters, 2002 , vol. 43, # 2 p. 311 - 313
反应条件
ammonium formate; palladium on activated charcoal in methanol T=20°C; Hydrogenolysis; 0.166667 h;
参考文献
Gowda; Rajesh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 7 p. 504 - 508
反应条件
3-(4,8-dimethoxy-1-naphthyl)-propionic acid; ascorbic acid powder in ethanol 2 h; Irradiation;
参考文献
Hamada, Tatsuo; Nishida, Atsushi; Yonemitsu, Osamu
Journal of the American Chemical Society, 1986 , vol. 108, # 1 p. 140 - 145
反应条件
sodium hydroxide; 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran; water T=0°C; pH=12; Product distribution / selectivity;
参考文献
WO2008/14811 A1, ;
Page/Page column 13-14 ;
反应条件
bis(tri-n-butyltin)oxide in toluene T=70°C; 36 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 995 - 999
反应条件
1: 1N NaOH 2: 79 percent / ascorbic acid, 3-(4,8-dimethoxy-1-naphthyl)-propionic acid / aq. ethanol / 2 h / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, # 1 p. 140 - 145
反应条件
sodium hydroxide in isopropyl alcohol Ambient temperature;
参考文献
Belagali, Shiddappa L.; Mathew, Thankamma; Himaja, M.; Kocienski, Philip
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 1 p. 45 - 47
反应条件
1: 1N NaOH 2: 79 percent / ascorbic acid, 3-(4,8-dimethoxy-1-naphthyl)-propionic acid / aq. ethanol / 2 h / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, # 1 p. 140 - 145
反应条件
tri-n-butyl-tin hydride; bis-triphenylphosphine-palladium(II) chloride in dichloromethane Ambient temperature;
参考文献
Guibe, F.; Dangles, O.; Balavoine, G.
Tetrahedron Letters, 1986 , vol. 27, # 21 p. 2365 - 2368
反应条件
1: 89 percent / aq. NaOH / 2-methyl-propan-2-ol / Ambient temperature 2: H2 / 5percent Pd/C / methanol; H2O / 24 h / 2585.7 Torr View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 5 p. 914 - 934