N-alpha-叔丁氧羰基-L-赖氨酸合成路线 （共 44 条）
反应条件
Bacillus cereus recombinant His-tagged alkaline D-peptidase; water; 2-[4-(2-hydroxyethyl)-1-piperazinyl] ethanesulfonic acid in N,N-dimethyl-formamide T=30°C; pH=8.0; Enzymatic reaction; Reactivity;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 29 p. 5456 - 5460
反应条件
piperidine; N,N-dimethyl-formamide 0.05 h;
参考文献
Tetrahedron Letters, , vol. 33, # 3 p. 397 - 400
反应条件
in water T=25°C; trypsin; Product distribution;
参考文献
Journal of Medicinal Chemistry, , vol. 24, # 5 p. 479 - 480
反应条件
(i) aq. NaOH, dioxane, (ii) H2, Pd-C, aq. MeOH; Multistep reaction;
参考文献
Helvetica Chimica Acta, , vol. 46, p. 870 - 889
反应条件
1: Py, aq. NaOH 2: aq. CF3CO2H, anisole View Scheme
参考文献
Bodanszky,M.; Fagan,D.T.
Journal of the American Chemical Society, 1977 , vol. 99, # 1 p. 235 - 239
反应条件
in N,N-dimethyl-formamide 120 h; Ambient temperature; Yield given;
参考文献
Acosta, C. Kirk; Bahr, Martin L.; Burdett, James E.; Cessac, James W.; Martinez, Rudy A.; et al.
Journal of Chemical Research, Miniprint, 1991 , # 5 p. 914 - 934
反应条件
sodium cyanoborohydride in water T=37°C; 132 h;
参考文献
Walton, Donald J.; Ison, Edward R.; Szarek, Walter A.
Carbohydrate Research, 1984 , vol. 128, p. 37 - 50
反应条件
T=37°C; pH=7.4; 168 h; aq. phosphate buffer;
参考文献
Smuda, Mareen; Voigt, Michael; Glomb, Marcus A.
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6458 - 6464
反应条件
air T=37°C; Maillard reaction; pH=7.4; 168 h; aq. phosphate buffer;
参考文献
Smuda, Mareen; Voigt, Michael; Glomb, Marcus A.
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6458 - 6464
反应条件
1.1: 85 percent / (benzotriazolyloxy)tris(Me2NH)phosphonium PF6(-); NaHCO3 / dimethylformamide / 12 h / 20 °C 2.1: NaH / tetrahydrofuran / 0.25 h / 20 °C 2.2: 95 percent / tetrahydrofuran / 5 h / 20 °C 3.1: 96 percent / H2 / 10 percent Pd/C / ethanol / 20 °C View Scheme
参考文献
Amblard, Muriel; Daffix, Isabelle; Berge, Gilbert; Calmes, Monique; Dodey, Pierre; Pruneau, Didier; Paquet, Jean-Luc; Luccarini, Jean-Michel; Belichard, Pierre; Martinez, Jean
Journal of Medicinal Chemistry, 1999 , vol. 42, # 20 p. 4193 - 4201
