1: N-(tert-butoxycarbonyl)-N-methylglycine With sodium hydride in tetrahydrofuran; mineral oil T=20°C; 0.166667 h; 2: methyl iodide in tetrahydrofuran; mineral oil T=60°C; 10 h;
参考文献
Ryakhovsky, Vladimir V.; Ivanov, Andrey S.
Tetrahedron, 2012 , vol. 68, # 35 p. 7070 - 7076
1: With 4-methyl-morpholine; isobutyl chloroformate in ethylene glycol dimethyl ether T=-15°C; 0.0166667 h; 2: With sodium tetrahydroborate in ethylene glycol dimethyl ether; water T=-15°C;
参考文献
McCusker, Kevin P.; Klinman, Judith P.
Tetrahedron Letters, 2009 , vol. 50, # 6 p. 611 - 613
