N-Boc-L-缬氨酸合成路线 （共 134 条）
反应条件
sodium hydroxide in N,N-dimethyl-formamide
参考文献
Justus Liebigs Annalen der Chemie, , vol. 716, p. 216 - 218
反应条件
sodium hydroxide in N,N-dimethyl-formamide
参考文献
Justus Liebigs Annalen der Chemie, , vol. 716, p. 175 - 185
反应条件
triethylamine 1.) dioxane, water, room temp., 30 min, 2.) 20 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 47, # 14 p. 2697 - 2700
反应条件
N+C5AlaHis2C16; phosphate buffer pH=7.47; in water T=15 - 40°C; enantioselectivity in ester hydrolysis; other micelle- and vesicle- catalysts; ΔH (excit.); ΔS (excit.); ΔG (excit.);; Rate constantKineticsMechanism;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 1 p. 172 - 180
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2305 - 2308
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2632 - 2636
反应条件
Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 118, # 2 p. 468 - 482
反应条件
1: 91 percent / NaH / tetrahydrofuran / 24 h / Ambient temperature 2: 98 percent / diethyl ether / 0 °C 3: 92 percent / HCl / dioxane / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 16 p. 5542 - 5549
反应条件
4-methyl-morpholine; ammonium hydroxide; isobutyl chloroformate in tetrahydrofuran T=-20 - 25°C; 16 h;
参考文献
Lefranc, David; Ciufolini, Marco A.
Angewandte Chemie, International Edition, 2009 , vol. 48, # 23 p. 4198 - 4201
反应条件
1: 1.) Et3N, EtOCOCl, 2.) NaBH4 / 1.) THF, 0 deg C, 0.25 h, 2.) H2O, 0 deg C, 0.5 h, room temperature, 2 h 2: Et3N, DMAP / CH2Cl2 / Ambient temperature 3: dimethylformamide / 24 h / Ambient temperature 4: 6 M HCl / 12 h / Heating View Scheme
参考文献
Sutherland, Andrew; Willis, Christine L.
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7764 - 7769
