N,N-二异丙基亚磷酰胺二叔丁酯合成路线 （共 4 条）
反应条件
triethylamine in diethyl ether T=0 - 20°C; 3.25 h;
参考文献
US7018987 B1, ;
Page/Page column 9 ;
反应条件
N,N-diisopropylamine tetrazolide 3 h;
参考文献
Helvetica Chimica Acta, , vol. 74, # 6 p. 1314 - 1328
反应条件
1: PCl3 / diethyl ether / 3 h / 20 °C 2: Et3N / diethyl ether / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 164, p. 277 - 291
反应条件
1: With 1H-tetrazole in tetrahydrofuran
T=20°C; 0.333333 h;
2: With 3-chloro-benzenecarboperoxoic acid in tetrahydrofuran; dichloromethane
T=-70 - 20°C; 0.0833333 h;
参考文献
Arizona Broad of Regents acting for and on behalf of Arizona State University
Patent: US7018987 B1, 2006 ;
Location in patent: Page/Page column 12-13 ;
