3-((4-溴苯基)硫代)丙酸合成路线 （共 10 条）
反应条件
PPA 0.0333333 h; microwave irradiation;
参考文献
Li, Ji-Tai; Li, Hong-Ya; Li, Hui-Zhang; Xiao, Li-Wei
Journal of Chemical Research, 2004 , # 6 p. 394 - 395
反应条件
sodium hydroxide; sodium carbonate in water
参考文献
Sankyo Company Limited
Patent: EP1031572 A1, 2000 ;
反应条件
1: With sodium hydroxide in water
1 h; Heating / reflux;
2: With hydrogenchloride; water
pH=~ 3;
参考文献
THE WALTER AND ELIZA HALL INSTITUTE OF MEDICAL RESEARCH
Patent: WO2009/39553 A1, 2009 ;
Location in patent: Page/Page column 93-94 ;
反应条件
1: p-bromophenyl mercaptan With sodium hydroxide in water
2: sodium 3-chloropropanoate in water
T=20°C; 4 h; Reflux;
3: With hydrogenchloride in water
T=20°C; pH=2;
参考文献
Okaecwe, Thokozile; Swanepoel, Abraham J.; Petzer, Anel; Bergh, Jacobus J.; Petzer, Jacobus P.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4336 - 4347
参考文献
Hurd; Hayao
Journal of the American Chemical Society, 1954 , vol. 76, p. 5065,5067
反应条件
pyridine; quinoline; nickel dichloride
1 h; Heating;
参考文献
Gogia, Santosh; Sirohi, Reenu; Gupta, Suman; Kishore; Joshi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 5 p. 1008 - 1011
反应条件
0.0666667 h; microwave irradiation;
参考文献
Li, Ji-Tai; Li, Hong-Ya; Li, Hui-Zhang; Xiao, Li-Wei
Journal of Chemical Research, 2004 , # 6 p. 394 - 395
反应条件
sodium hydroxide
1.) H2O, room temperature, 30 min, 2.) room temperature, 48 h; Yield givenMultistep reaction;
参考文献
Johnson, Alan T.; Wang, Liming; Standeven, Andrew M.; Escobar, Maria; Chandraratna, Roshantha A.S.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 7 p. 1321 - 1338
参考文献
Friedmann
B. Ph. P., 1904 , vol. 4, p. 501
参考文献
Friedmann
B. Ph. P., 1904 , vol. 4, p. 500
