1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
triethylamine; sodium iodide in acetonitrile 0.25 h; Ambient temperature;
参考文献
Lin, Ji-Mao; Liu, Ben-Sheng
Synthetic Communications, 1997 , vol. 27, # 5 p. 739 - 749
反应条件
1: (S)-(-)-methyl p-tolyl sulfoxide With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: PhC(O)TMS in tetrahydrofuran; hexane T=-78°C; 2 h; regioselective reaction;
参考文献
Honda, Mitsunori; Nakajima, Tadashi; Okada, Maiko; Yamaguchi, Keita; Suda, Mitsuhiro; Kunimoto, Ko-Ki; Segi, Masahito
Tetrahedron Letters, 2011 , vol. 52, # 29 p. 3740 - 3742
反应条件
{[pyridine-2,6-(2,6-iPr2Ph-N=C(CH3))2]Rh(I)}(1+) in dichloromethane
参考文献
Dias; Brookhart; White
Journal of the American Chemical Society, 2001 , vol. 123, # 10 p. 2442 - 2443
反应条件
potassium cyanide; 2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Nakamura, Eiichi; Hashimoto, Koichi; Kuwajima, Isao
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 805 - 808
反应条件
molecular sieve; tris(dimethylamino)-sulphonium difluorotrimethylsilicate in tetrahydrofuran T=20°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 8 p. 2498 - 2503
反应条件
triethylamine in diethyl ether 2 h; Ambient temperature;
参考文献
Emde, Herbert; Goetz, Andreas; Hofmann, Karin; Simchen, Gerhard
Liebigs Annalen der Chemie, 1981 , # 9 p. 1643 - 1657
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 2 h;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
[Bu4N]+[(MeO)2P(O)O]- in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Prakash, G.K. Surya; Panja, Chiradeep; Vaghoo, Habiba; Surampudi, Vijayalakshmi; Kultyshev, Roman; Mandal, Mihirbaran; Rasul, Golam; Mathew, Thomas; Olah, George A.
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 6806 - 6813
反应条件
1: diiodomethane With zinc; PbCl2 in tetrahydrofuran T=25°C; 2 h; 2: S-4-nitrophenyl thiobenzoate With trifuran-2-yl-phosphane; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran T=0°C; 0.25 h; 3: chloro-trimethyl-silane in tetrahydrofuran T=25°C; 0.25 h; Further stages.;
参考文献
Chemical Communications, , # 45 p. 4761 - 4763
反应条件
1,1,1,3,3,3-hexamethyl-disilazane in tetrachloromethane T=10°C; 6 h; Yields of byproduct given;
参考文献
Miller, R. D.; McKean, D. R.
Synthetic Communications, 1982 , vol. 12, # 4 p. 319 - 322
