1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
silica gel 1.) 110 deg C, 15 h, 2.) CHCl3, r.t., 20 h; Multistep reaction. Yields of byproduct given;
参考文献
Lociuro, Sergio; Pellacani, Lucio; Tardella, Paolo A.
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 593 - 596
反应条件
1: ammonium hexanitratocerate(IV); KOH / methanol / 0.25 h / -78 °C 2: DBU / CH2Cl2 / 20 °C View Scheme
参考文献
Hayashi, Masaji; Mukaiyama, Teruaki
Chemistry Letters, 1987 , p. 1283 - 1286
反应条件
T=40°C; 32 h; Irradiation;
参考文献
Voronkov, M. G.; Rakhlin, V. I.; Khangazeev, S. Kh.; Mirskov, R. G.; Dneprovskii, A. S.
Doklady Chemistry, 1981 , vol. 259, p. 386 - 388
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 259, # 6 p. 1364 - 1366
反应条件
lithium aluminium tetrahydride; oxygen 1) chlorobenzene, heating; Multistep reaction. Yields of byproduct given;
参考文献
Suprun
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 1 p. 52 - 58
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature;
参考文献
Takeda, Kazuyoshi; Ayabe, Akira; Kawashima, Hideki; Harigaya, Yoshihiro
Tetrahedron Letters, 1992 , vol. 33, # 7 p. 951 - 952
反应条件
silver trifluoromethanesulfonate in 1,2-dichloro-ethane 6 h; Heating;
参考文献
Takeda, Kazuyoshi; Torii, Katsumi; Ogura, Haruo
Tetrahedron Letters, 1990 , vol. 31, # 2 p. 265 - 266
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.; Pombo-Villar, Esteban
Tetrahedron, 2005 , vol. 61, # 45 p. 10757 - 10773
反应条件
1: 63 percent / nitromethane; CH2Cl2 / -50 deg C, 30 min to r.t., 18 h 2: 75 percent / HgCl2/HgO / methanol; H2O / 2 h / Heating View Scheme
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 5 p. 1798 - 1808
反应条件
calcine-dried potassium fluoride; DTPP-F6 Yield given. Multistep reaction;
参考文献
Kitazume, Tomoya; Ishikawa, Nobuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 7 p. 2064 - 2066
反应条件
fluorine in various solvent(s) T=-78°C; 3.5 h;
参考文献
Purrington, Suzane T.; Lazaridis, Nicholas V.; Bumgardner, Carl L.
Tetrahedron Letters, 1986 , vol. 27, # 24 p. 2715 - 2716
