1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
1: With iodotoluene difluoride; boron trifluoride diethyl etherate in dichloromethane T=-78°C; 2 h; 2: With triethylamine hydrofluoric acid in dichloromethane
参考文献
Sato, Saeko; Yoshida, Masanori; Hara, Shoji
Synthesis, 2005 , # 15 art. no. F18704SS, p. 2602 - 2605
反应条件
1: With iodotoluene difluoride; boron trifluoride diethyl etherate in dichloromethane T=-78°C; 2 h; 2: With triethylamine tris(hydrogen fluoride) in dichloromethane 1 h;
参考文献
Sato, Saeko; Yoshida, Masanori; Hara, Shoji
Synthesis, 2005 , # 15 art. no. F18704SS, p. 2602 - 2605
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
copper(I) oxide in further solvent(s) solvent : (CH3)2CHCN;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.1, page 48 - 120
参考文献
Zhdankin, Viktor V.
Tetrahedron Letters, 1990 , vol. 31, # 34 p. 4821 - 4824
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Kuehl, Chris J.; Simonsen, Angela J.
Tetrahedron Letters, 1995 , vol. 36, # 13 p. 2203 - 2206
反应条件
tris(cetyl)pyridinium 12-tungstophosphate; dihydrogen peroxide in dichloromethane T=20°C; oxidative cleavage; 0.5 h;
参考文献
Sakaguchi, Satoshi; Yamamoto, Yumiko; Sugimoto, Takuma; Yamamoto, Hiroyo; Ishii, Yasutaka
Journal of Organic Chemistry, 1999 , vol. 64, # 16 p. 5954 - 5957
