1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
XeF2 in acetonitrile T=20°C; 1 h;
参考文献
Organic Letters, , vol. 1, # 10 p. 1591 - 1594
反应条件
AcOF in chloroform; acetic acid; acetonitrile
参考文献
Journal of Fluorine Chemistry, , vol. 61, # 1.2 p. 141 - 146
反应条件
1: With iodotoluene difluoride; boron trifluoride diethyl etherate in dichloromethane T=-78°C; 2 h; 2: With triethylamine hydrofluoric acid in dichloromethane
参考文献
Synthesis, , # 15 art. no. F18704SS, p. 2602 - 2605
反应条件
1: With iodotoluene difluoride; boron trifluoride diethyl etherate in dichloromethane T=-78°C; 2 h; 2: With triethylamine tris(hydrogen fluoride) in dichloromethane 1 h;
参考文献
Synthesis, , # 15 art. no. F18704SS, p. 2602 - 2605
反应条件
(i) Zn-Cu, (ii) /BRN= 605303/; Multistep reaction;
参考文献
Ryu,I. et al.
Chemistry Letters, 1976 , p. 93 - 94
反应条件
1: 77 percent / ZnBr2 View Scheme
参考文献
Ager, David J.
Tetrahedron Letters, 1983 , vol. 24, # 4 p. 419 - 422
反应条件
[ReCl(N2)(PMe2Ph)4] in N,N-dimethyl-formamide Cyclization; addition; Heating;
参考文献
Koga, Yuji; Kusama, Hiroyuki; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 2 p. 475 - 482
反应条件
(PyCOO)3Mn in N,N-dimethyl-formamide Ambient temperature; Yields of byproduct given;
参考文献
Narasaka, Koichi; Miyoshi, Norikazu; Iwakura, Kazunori; Okauchi, Tatsuo
Chemistry Letters, 1989 , p. 2169 - 2172
反应条件
1: 10.7 g / TiCl4 / CH2Cl2 / 6 h / Ambient temperature 2: p-TsOH / benzene / 5.25 h / Heating 3: 57 percent / 1.) -23 deg C, 5.25 h, 2.) room temperature, 45 min 4: 90 percent / Raney nickel / ethanol / 20 h / 90 °C 5: 98 percent / HBF4*Et2O / CH2Cl2 / 1.5 h / Ambient temperature 6: 62 percent / MCPBA, tert-butyl-4-hydroxy-5-methylphenylsulfide / N,N-dimethyl-acetamide / 60 °C View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride; potassium bromide 1.) CH2Cl2, room temperature, 10 h, 2.) DMF, room temperature, 24 h; Yield given. Multistep reaction;
参考文献
Yoshikawa, Takashi; Mori, Seiji; Shindo, Mitsuru
Tetrahedron, 2009 , vol. 65, # 43 p. 8832 - 8838
