1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
Yield given. Multistep reaction;
参考文献
Danheiser, Rick L.; Miller, Raymond F.; Brisbois, Ronald G.; Park, Saung Z.
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1959 - 1964
反应条件
TeCl4 in dichloromethane 2 h; Ambient temperature;
参考文献
Tani, Hiroyuki; Inamasu, Tokuo; Masumoto, Kazunori; Tamura, Rui; Shimizu, Hiroshi; Suzuki, Hitomi
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 67, # 1-4 p. 261 - 266
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 0.333333 h;
参考文献
Ali, Ibrahim A. I.; El Ashry, El Sayed H.; Schmidt, Richard R.
Tetrahedron, 2004 , vol. 60, # 22 p. 4773 - 4780
反应条件
trimethylsilyl iodide in dichloromethane T=-78°C; 1 h;
参考文献
Sakurai, Hideki; Sasaki, Koshi; Hosomi, Akira
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 10 p. 3195 - 3196
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
titanium tetrachloride in dichloromethane T=-70°C; 1 h;
参考文献
Mulzer, Johann; Bruentrup, Gisela; Hartz, Georg; Kuehl, Uwe; Blaschek, Ursula; Boehrer, Gerald
Chemische Berichte, 1981 , vol. 114, # 11 p. 3701 - 3724
反应条件
in toluene T=100°C; 1 h;
参考文献
Heterocycles, , vol. 36, # 9 p. 2139 - 2146
反应条件
indium(III) chloride in dichloromethane T=20°C; 2 h;
参考文献
Nishimoto, Yoshihiro; Yasuda, Makoto; Baba, Akio
Organic Letters, 2007 , vol. 9, # 24 p. 4931 - 4934
反应条件
silver trifluoromethanesulfonate in dichloromethane 2 h; Ambient temperature;
参考文献
Takeda, Kazuyoshi; Torii, Katsumi; Ogura, Haruo
Tetrahedron Letters, 1990 , vol. 31, # 2 p. 265 - 266
反应条件
pyridine; silver trifluoromethanesulfonate; trichloromethyl chloroformate multistep reaction, other solvent, other benzylic alcohols, other silyl enol ethers; Product distribution;
参考文献
Takeda, Kazuyoshi; Ayabe, Akira; Kawashima, Hideki; Harigaya, Yoshihiro
Tetrahedron Letters, 1992 , vol. 33, # 7 p. 951 - 952