1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
iodosylbenzene; boron trifluoride diethyl etherate T=-70°C; 3.5 h;
参考文献
Journal of Organic Chemistry, , vol. 52, # 1 p. 150 - 153
反应条件
lead(IV) acetate 2 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 17, # 6 p. 709 - 714
反应条件
indium(III) chloride in dichloromethane T=0°C; 1.5 h;
参考文献
Russowsky; Petersen; Godoi; Pilli
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9939 - 9942
反应条件
NiCl2((PPh3)P)2 1.) ether, room temp., 2.) benzene, reflux; Yield given. Multistep reaction;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
Ni(PCy3)2Cl2 in toluene T=30°C; Kumada-Tamao-Corriu coupling; 1 h; Inert atmosphere;
参考文献
Zhao, Fei; Yu, Da-Gang; Zhu, Ru-Yi; Xi, Zhenfeng; Shi, Zhang-Jie
Chemistry Letters, 2011 , vol. 40, # 9 p. 1001 - 1003
反应条件
in acetonitrile 1 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 62, # 9 p. 2742 - 2751
反应条件
1: CH2Cl2 / -78 °C
2: 63 percent / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
trimethylsilyl trifluoromethanesulfonate; iodosylbenzene in dichloromethane
Ambient temperaturevar. trimethylsilyl ketene acetals of esters/lactones;
参考文献
Moriarty, Robert M.; Epa, Widanagamage R.; Prakash, Om
Journal of Chemical Research - Part S, 1997 , # 7 p. 262 - 263
反应条件
in dichloromethane
2 h; Ambient temperature;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Awasthi, Alok K.; Epa, W. Ruwan; Prakash, Indra
Journal of Organic Chemistry, 1989 , vol. 54, # 5 p. 1101 - 1104
反应条件
ammonium cerium(IV) nitrate; 4 A molecular sieve in acetonitrile
T=-23°C; 0.333333 h;
参考文献
Narasaka, Koichi; Arai, Noriyoshi; Okauchi, Tatsuo
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 2995 - 3003