1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
potassium fluoride in dichloromethane
1.5 h; Ambient temperaturevarious additives and solvents, various reaction conditions; Product distribution;
参考文献
Umemoto, Teruo; Gotoh, Yoshihiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3823 - 3826
反应条件
1: CuCl
2: 87 percent / tributyltin hydride, AIBN / benzene / 1 h / Heating; other β-chloro-β-trifluoromethyl-acroleines (-vinylketones)
View Scheme
参考文献
Laurent; Lesniak
Tetrahedron Letters, 1992 , vol. 33, # 52 p. 8091 - 8092
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Umemoto, Teruo; Gotoh, Yoshihiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3823 - 3826
反应条件
1: With N,N-bis(perfluoromethanesulfonyl)squaramide in acetonitrile
T=20°C; Mukaiyama aldol reaction; 2 h;
2: With hydrogenchloride in water; acetonitrile
0.166667 h;
参考文献
Cheon, Cheol Hong; Yamamoto, Hisashi
Tetrahedron, 2010 , vol. 66, # 24 p. 4257 - 4264
反应条件
1: mischmetall tribromide*(thf)x / CH2Cl2 / 48 h / 20 °C
2: aq. HCl / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Lannou, Marie-Isabelle; Helion, Florence; Namy, Jean-Louis
Tetrahedron, 2003 , vol. 59, # 52 p. 10551 - 10565
反应条件
water; cesium fluoride
1.) 25 deg C, 10 min; Yield given. Multistep reaction;
参考文献
Boyer, J.; Corriu, R. J. P.; Perz, R.; Reye, C.
Journal of Organometallic Chemistry, 1980 , vol. 184, # 2 p. 157 - 166
反应条件
in dichloromethane
2 h; Ambient temperature;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Awasthi, Alok K.; Epa, W. Ruwan; Prakash, Indra
Journal of Organic Chemistry, 1989 , vol. 54, # 5 p. 1101 - 1104
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Kuehl, Chris J.; Simonsen, Angela J.
Journal of Organic Chemistry, 1996 , vol. 61, # 23 p. 8272 - 8276
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Kuehl, Chris J.; Simonsen, Angela J.
Tetrahedron Letters, 1995 , vol. 36, # 13 p. 2203 - 2206
反应条件
tin(IV) chloride in tetrahydrofuran
T=-35 - -30°C;
参考文献
Ishihara, Takashi; Shinjo, Hiroshi; Inoue, Yoshihisa; Ando, Teiichi
Journal of Fluorine Chemistry, 1983 , vol. 22, p. 1 - 20
