1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
lithium iodide in tetrahydrofuran; hexane T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 49, # 37 p. 8343 - 8358
反应条件
in tetrahydrofuran; dimethyl-ether T=-110°C;
参考文献
Tetrahedron Letters, , vol. 24, # 45 p. 4907 - 4910
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=100°C; 12 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 234, # 3 p. 367 - 374
反应条件
C6F5SiMe3; copper diacetate; 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran T=-78°C; Inert atmosphere;
参考文献
Synlett, , # 4 art. no. D30809ST, p. 615 - 617
反应条件
in chloroform-d1 Sonication; room temp., 2.5 h; chromy. (silica gel) isolation of (Ph3P)AuCl); (1)H-NMR;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, p. 3649 - 3652
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 5 h; other α-halo ketones; var. temp., solvents and catalyst; effects of the temperature and catalyst on the yield and distribution of the products; Product distribution;
参考文献
Kosugi, Masanori; Ohya, Takao; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 11 p. 3539 - 3540
反应条件
in dichloromethane 1.) 30 min, -30 deg C; 2.) 15 h, 20 deg C;
参考文献
Schroth, Werner; Jahn, Ullrich; Stroehl, Dieter
Chemische Berichte, 1994 , vol. 127, # 10 p. 2013 - 2022
反应条件
1: diethyl ether 2: HgI2 View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 11, p. 35 - 48
反应条件
in tetrahydrofuran T=20°C;
参考文献
Tetrahedron, , vol. 49, # 37 p. 8343 - 8358
反应条件
in tetrahydrofuran T=20°C; 1 h;
参考文献
Nakajima, Tadashi; Segi, Masahito; Sugimoto, Fumitosi; Hioki, Reiko; Yokota, Seiko; Miyashita, Kiyoshi
Tetrahedron, 1993 , vol. 49, # 37 p. 8343 - 8358