1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
potassium tert-butylate
参考文献
Katritzky, Alan R.; Hayden, Amy E.; Kirichenko, Kostyantyn; Pelphrey, Phillip; Ji, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5108 - 5111
反应条件
iodine in methanol
T=20°C; 0.166667 h;
参考文献
Lee, Byoung Se; Mahajan, Suresh; Janda, Kim D.
Synlett, 2005 , # 8 art. no. S01705ST, p. 1325 - 1327
反应条件
bismuth trifluoromethanesulphonate in acetonitrile
T=25°C;
参考文献
Ollevier, Thierry; Nadeau, Etienne
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 19 p. 3126 - 3134
反应条件
trifluorormethanesulfonic acid in isopropyl alcohol
T=20°C;
参考文献
Akiyama, Takahiko; Nakashima, Saeko; Yokota, Koji; Fuchibe, Kohei
Chemistry Letters, 2004 , vol. 33, # 7 p. 922 - 923
反应条件
benzaldehyde; trifluoroacetic acid in 1-methyl-pyrrolidin-2-one
T=-40 - -25°C; Mannich reaction; 3 h;
参考文献
Hayashi, Yujiro; Urushima, Tatsuya; Shoji, Mitsuru; Uchimaru, Tadafumi; Shiina, Isamu
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 11-13 p. 1595 - 1604
反应条件
tetrafluoroboric acid; water; sodium lauryl sulfate
T=25°C; Condensation; 2 h;
参考文献
Akiyama, Takahiko
Synlett, 1999 , # 9 p. 1426 - 1428
反应条件
1: pivalaldehyde With N,N-bis(perfluoromethanesulfonyl)squaramide in acetonitrile
T=20°C; 0.166667 h; Inert atmosphere;
2: [(1-phenyl-1-ethenyl)oxy]trimethylsilane in acetonitrile
T=20°C; Mukaiyama aldol reaction; 2 h; Inert atmosphere;
3: With hydrogenchloride; water
T=20°C; Mukaiyama aldol reaction; 0.5 h; Inert atmosphere;
参考文献
Cheon, Cheol Hong; Yamamoto, Hisashi
Tetrahedron, 2010 , vol. 66, # 24 p. 4257 - 4264
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78°C;
参考文献
Mukai; Hashizume; Nagami; Hanaoka
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 6 p. 1509 - 1512
反应条件
1: 90 percent / <ZrCp2(CF2SO3)2THF> / CD3NO2 / 0.12 h / 25 °C
2: trifluoroacetic acid, H2O / nitromethane / 0 °C
View Scheme
参考文献
Hollis, T. Keith; Odenkirk, William; Robinson; Whelan, John; Bosnich
Tetrahedron, 1993 , vol. 49, # 25 p. 5415 - 5430
反应条件
in dichloromethane
T=0°C; 0.5 h;
参考文献
Itoh, Takashi; Miyazaki, Michiko; Nagata, Kazuhiro; Hasegawa, Hiroshi; Ohsawa, Akio; Nakamura, Kazuo T.
Heterocycles, 1998 , vol. 47, # 1 p. 125 - 128
