1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
in acetonitrile
T=0°C; 1 h;
参考文献
Akiba, Kin-ya; Nakatani, Masayuki; Wada, Makoto; Yamamoto, Yohsuke
Journal of Organic Chemistry, 1985 , vol. 50, # 1 p. 63 - 68
反应条件
aluminium trichloride in dichloromethane
1 h; 1.) -45 deg C, 2.) 0 deg C;
参考文献
Dawe, Robert David; Fraser-Reid, Bert
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 522 - 528
反应条件
boron trifluoride diethyl etherate in dichloromethane
1.) -45 deg C, 2.) 0 deg C;
参考文献
Dawe, Robert David; Fraser-Reid, Bert
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 522 - 528
反应条件
aluminium trichloride in dichloromethane
0.75 h; 1.) -45 deg C, 2.) 0 deg C; Yields of byproduct given;
参考文献
Dawe, Robert David; Fraser-Reid, Bert
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 522 - 528
反应条件
aluminium trichloride in dichloromethane
0.75 h; 1.) -45 deg C, 2.) 0 deg C; Yields of byproduct given;
参考文献
Dawe, Robert David; Fraser-Reid, Bert
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 522 - 528
反应条件
[Mo(II)(CO)4Br2]2 in dichloromethane
T=20°C; 0.166667 h;
参考文献
Malkov, Andrei V.; Farn, Benjamin P.; Hussain, Nigel; Kocovsky, Pavel
Collection of Czechoslovak Chemical Communications, 2001 , vol. 66, # 12 p. 1735 - 1745
参考文献
Dawe, Robert David; Fraser-Reid, Bert
Journal of the Chemical Society, Chemical Communications, 1981 , # 22 p. 1180 - 1181
反应条件
1: 71 percent / Na2CO3 / acetonitrile / 20 h / Ambient temperature
2: 70 percent / Fe3(CO)12 / toluene / 20 h / 100 °C
View Scheme
参考文献
Nakanishi, Saburo; Otsuji, Yoshio; Itoh, Keiji; Hayashi, Nobuaki
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3595 - 3600
反应条件
zinc(II) chloride in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts alkylation; 16 h; Inert atmosphere;
参考文献
Smith, Austin G.; Johnson, Jeffrey S.
Organic Letters, 2010 , vol. 12, # 8 p. 1784 - 1787
反应条件
1: 69 percent / ZnBr2
2: 77 percent / NaIO4
3: 54 percent / NaI, Et3N / acetonitrile / 6 h / 100 °C
View Scheme
参考文献
Fleming, Ian; Iqbal, Javed
Tetrahedron Letters, 1983 , vol. 24, # 28 p. 2913 - 2916
