1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
Yields of byproduct given;
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
lithium perchlorate; sodium carbonate in acetonitrile
参考文献
Renaud, Roger N.; Stephens, Campbell J.; Brochu, Gaetan
Canadian Journal of Chemistry, 1984 , vol. 62, p. 565 - 569
反应条件
1: 10.7 g / TiCl4 / CH2Cl2 / 6 h / Ambient temperature
2: p-TsOH / benzene / 5.25 h / Heating
3: 57 percent / 1.) -23 deg C, 5.25 h, 2.) room temperature, 45 min
4: 90 percent / Raney nickel / ethanol / 20 h / 90 °C
View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
反应条件
1: 10.7 g / TiCl4 / CH2Cl2 / 6 h / Ambient temperature
2: p-TsOH / benzene / 5.25 h / Heating
3: 57 percent / 1.) -23 deg C, 5.25 h, 2.) room temperature, 45 min
4: 90 percent / Raney nickel / ethanol / 20 h / 90 °C
5: 98 percent / HBF4*Et2O / CH2Cl2 / 1.5 h / Ambient temperature
View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
反应条件
bismuth trifluoromethanesulphonate in dichloromethane
T=-70°C; 120 h;
参考文献
Roux, C. Le; Ciliberti, L.; Laurent-Robert, H.; Laporterie, A.; Dubac, J.
Synlett, 1998 , # 11 p. 1249 - 1251
反应条件
Et3Si[B(C6F5)4] in toluene
T=-78°C; Mukaiyama aldol reaction; 1 h;
参考文献
Hara, Kenji; Akiyama, Ryuto; Sawamura, Masaya
Organic Letters, 2005 , vol. 7, # 25 p. 5621 - 5623
反应条件
1: 92 percent / dioxane / 5 h / 25 °C
2: NaOH / tetrahydrofuran / 12 h / Heating
3: 78 percent / various solvent(s) / 0.25 h / 200 °C
View Scheme
参考文献
Boger, Dale L.; Coleman, Robert S.; Panek, James S.; Yohannes, Daniel
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4405 - 4409
