1-苯基-1-三甲基甲硅氧基乙烯合成路线 （共 431 条）
反应条件
Ph3C+ClO4- in dichloromethane
T=-78°C; 0.166667 h;
参考文献
Mukaiyama, Teruaki; Kobayashi, Shu; Murakami, Masahiro
Chemistry Letters, 1984 , p. 1759 - 1762
反应条件
1: benzaldehyde With chiral water-tolerant In(III)-camphorsulfonate complex in water
T=20°C; Mannich reaction;
2: 4-chloro-aniline in water
T=20°C;
3: [(1-phenyl-1-ethenyl)oxy]trimethylsilane in water
T=20°C; 24 h; Further stages.;
参考文献
Xiao, Jian; Loh, Teck-Peng
Synlett, 2007 , # 5 p. 815 - 817
反应条件
TBPA+ in dichloromethane
T=20°C; Mannich reaction; 0.5 h;
参考文献
Jia, Xiao-Dong; Wang, Wen-Juan; Huo, Cong-De; Quan, Zheng-Jun; Ren, Yan; Wang, Xi-Cun
Synlett, 2010 , # 19 p. 2964 - 2968
反应条件
trimethylsilyl trifluoromethanesulfonate
1.) dichloromethane, 0 deg C, 10 min, 2.) dichloromethane, room temperature, 2 h; Yield given. Multistep reaction;
参考文献
Pilli, R. A.; Russowsky, D.
Journal of the Chemical Society, Chemical Communications, 1987 , # 14 p. 1053 - 1054
反应条件
hydrogenchloride; bismuth(III) chloride
1) CH2Cl2, 15 min, RT; 2) CH3OH, H2O; Yield given. Multistep reaction;
参考文献
Ohki, Hidenori; Wada, Makoto; Akiba, Kin-ya
Tetrahedron Letters, 1988 , vol. 29, # 37 p. 4719 - 4722
反应条件
Fe(η5-C5H5)2(PF6); 4 A molecular sieve in acetonitrile
Ambient temperature;
参考文献
Narasaka, Koichi; Arai, Noriyoshi; Okauchi, Tatsuo
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 2995 - 3003
反应条件
in nitromethane; dichloromethane
-50 deg C, 30 min to r.t., 18 h;
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 5 p. 1798 - 1808
反应条件
in nitromethane; dichloromethane
-50 deg C, 30 min to r.t., 18 h;
参考文献
Stahl, Ingfried
Chemische Berichte, 1985 , vol. 118, # 5 p. 1798 - 1808
反应条件
1: 60 percent / <ZrCp2(CF2SO3)2THF> / CD3NO2 / 19 h / 25 °C
2: trifluoroacetic acid, H2O / nitromethane / 0 °C
View Scheme
参考文献
Hollis, T. Keith; Odenkirk, William; Robinson; Whelan, John; Bosnich
Tetrahedron, 1993 , vol. 49, # 25 p. 5415 - 5430
反应条件
TeCl4 in dichloromethane
2 h; Ambient temperature;
参考文献
Tani, Hiroyuki; Inamasu, Tokuo; Masumoto, Kazunori; Tamura, Rui; Shimizu, Hiroshi; Suzuki, Hitomi
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 67, # 1-4 p. 261 - 266
